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  tri-nitro-phenol and purifying sulfuric acid

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Author Topic:   tri-nitro-phenol and purifying sulfuric acid
PEACE
A New Voice
posted December 16, 1999 07:54 AM     Click Here to See the Profile for PEACE   Click Here to Email PEACE     
i was thinking of attempting to make trinitriphenol from aspirin (acetylsalicylic acid) , sulfuric acid and potassium nitrate.

BUT I was looking for some advice on safety or even a tried method from someone in this forum? i read that this is very toxic and contains picric acid. Should i attempt to make this? i mean would anybody in here make it?

also if i boiled sulfuric acid until white fumes appeared approx. how concentrated would it be? enough to form the explosive above?

thanx
-PEACE


nbk2000
Moderator
posted December 16, 1999 09:46 AM     Click Here to See the Profile for nbk2000   Click Here to Email nbk2000     
Trinitrophenol and picric acid are the same thing! And yes it is toxic so don't eat it or touch it with bare skin. Also, don't inhale any of the fumes given off during the nitrate addition to the acid mix. Do all the heating and mixing outdoors.

Boiling sulfuric acid will concentrate it to above 90% which is more than adequate for making picric acid. My explosives section has several different process for making picric acid.

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"The knowledge that they fear is a weapon to be used against them." www.50megs.com/nbk2000



PEACE
A New Voice
posted December 16, 1999 05:52 PM     Click Here to See the Profile for PEACE   Click Here to Email PEACE     
hehhe shit i didnt know that!!!

thanks for the info nbk2000, and what would detonate this explosive effectively?
btw is trinitrophenol more powerful than TNT?

thanx
-PEACE


nbk2000
Moderator
posted December 16, 1999 08:23 PM     Click Here to See the Profile for nbk2000   Click Here to Email nbk2000     
AP or HMTD would work just fine. Just keep the picric away from metals if your going to keep it for any length of time. As for power, it's more powerful than TNT, but because of the expense and metal reactivity, it's no longer used by the military.

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"The knowledge that they fear is a weapon to be used against them." www.50megs.com/nbk2000



HMTD Factory
Frequent Poster
posted December 17, 1999 09:04 AM     Click Here to See the Profile for HMTD Factory     
Peace, you can wash your product with some
ammonia, it will get rid of the remaining acid, react the picric acid into Explosive D,
ammonium picrate, used in HEAP.


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